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    Inductively coupled plasma emission spectrometer

    ICP-6800S(Petrochemical)

    Model:ICP-6800S
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    Product description, technical parameters and configuration

    ICP-6800S Inductively Coupled Plasma Optical Emission Spectrometer(Petrochemical)

    Application Field

    Petrochemical Inductively Coupled Plasma Optical Emission SpectrometerICP6800S is a professional instrument for the petrochemical industry launched by Macylab Instruments. It can be used to determine more than 30 elements in crude oil, mainly for Fe.Na.Mg.Ni. V.Ca. Pb.Mo.Mn.Cr.Ca.Ba.As; also can be used to measure iron, manganese, lead, silicon in gasoline ,and the Wear elements of additive in lubricating oil, it also can be applied for multielement determination in base oils; for the determination of sodium in formaldehyde and the determination of oil field tracer.

     

    Application Environment

    CONTENT                                                   RANGE

    Shipping/Storage Ambient Temperature         15-25

    Shipping/Storage Relative Humidity               70

    Atmospheric pressure                                   86-106 kPa

    Power Supply                                              220±10V  50-60MHz

    Working Humidity                                        70

    Working Temperature                                  15-30

     

    Technical Parameter

    RFPower technical parameter:

    Circuit type: solid-state RF power supply, with function of automatch

    Frequency: 27.12MHz±0.05

    Frequency Stability: 0.1%

    Power Output: 800W—1500W

    Power Output Stability: 0.3%

    Escaped RF radiation: 30cm away from the instrument, electric field: E2V/m

     

    Sampling System Technical Parameter:

    Output working coil inner diameter :25mm

    Torque tube: Three concentric, external diameter 20mm

    Coaxial nebulizer:Outer diameter 6mm

    Double barrel atomizing chamber: Outer diameter 34mm

     

    Gas Flow Controls

    1. Plasma Argon Flowmeter:100-1000L/h (1.6-16L/min)

    2. Auxiliary Argon Flowmeter:10-100L/h (0.16-1.66L/min)

    3. Carrier Argon Flowmeter10-100L/h (0.16-1.66L/min)

    4.Oxygen Flowmeter:0-100ml/min (30-50ml/min) 

    5.Pressure Maintaining Valve0-0.4MPa

    6.Cooling Water:Temperature: 20-25, Rate of Flow>5L/min, Hydraulic Pressure>0.1MPa

     

    Spectrometer

    Optics:Czerny-Turner type

    Focal length: 1000 mm

    Grating: Ion Beam Etching Holographic Grating, 4320L/mm

    Reciprocal linear dispersion: 0.26nm/mm

    Resolution: 0.005nm (4320 line grating)

    Wavelength range: 4320 line grating:(180nm435) nm

    Minimum pace of stepping motor: 0.0006 nm

    Exit Slit:10μm;Entrance Slit:8μm

     

    Photoelectric Converter Performance

    Photomultiplier tube specification: R293

    Negative HV on PMT: 0-1000V;Stability: 0.05%

     

    Refrigeration System

    Refrigerating Swirling Fog Chamber:The use of imported silica gel collection technology can make the temperature drop to 20 degrees below zero

     

    Overall Performance

    Wavelength range of scanning: 185nm435nm(4320L/mm line grating)

    Repeatability: RSD(Relative Standard Deviation)1.5

    Stability: RSD(Relative Standard Deviation) 2

    Detection Limits (µg/L):

    Direct injection sampling and measure iron(Fe), manganese(Mn), lead(Pb) and silicon(Si) in gasoline.Analysis results:

    Element

    Fe

    Mn

    Pb

    Si

    Determination value/(mg/L)

    3.6

    17.5

    1.8

    2.4

    RSD/%

    0.56

    0.23

    1.38

    0.92

     

    Standard Additionand Recovery Rate:

    Number

    Standard Addition

    mg/L

    Fe

    Mn

    Pb

    Si

     

     

    Determination valuemg/L

    Recovery

    /%

    Determination valuemg/L

    Recovery

    /%

    Determination valuemg/L

    Recovery

    /%

    Determination valuemg/L

    Recovery

    /%

    1

    0.45

    0.436

    96.9

    0.468

    104.0

    0.432

    96.0

    0.465

    103.3

      2

    0.9

    0.887

    98.6

    0.913

    101.4

    0.868

    96.4

    0.919

    102.1

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