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Inductively coupled plasma emission spectrometer

ICP-6800S(Petrochemical)

Model:ICP-6800S
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Product description, technical parameters and configuration

ICP-6800S Inductively Coupled Plasma Optical Emission Spectrometer(Petrochemical)

Application Field

Petrochemical Inductively Coupled Plasma Optical Emission SpectrometerICP6800S is a professional instrument for the petrochemical industry launched by Macylab Instruments. It can be used to determine more than 30 elements in crude oil, mainly for Fe.Na.Mg.Ni. V.Ca. Pb.Mo.Mn.Cr.Ca.Ba.As; also can be used to measure iron, manganese, lead, silicon in gasoline ,and the Wear elements of additive in lubricating oil, it also can be applied for multielement determination in base oils; for the determination of sodium in formaldehyde and the determination of oil field tracer.

 

Application Environment

CONTENT                                                   RANGE

Shipping/Storage Ambient Temperature         15-25

Shipping/Storage Relative Humidity               70

Atmospheric pressure                                   86-106 kPa

Power Supply                                              220±10V  50-60MHz

Working Humidity                                        70

Working Temperature                                  15-30

 

Technical Parameter

RFPower technical parameter:

Circuit type: solid-state RF power supply, with function of automatch

Frequency: 27.12MHz±0.05

Frequency Stability: 0.1%

Power Output: 800W—1500W

Power Output Stability: 0.3%

Escaped RF radiation: 30cm away from the instrument, electric field: E2V/m

 

Sampling System Technical Parameter:

Output working coil inner diameter :25mm

Torque tube: Three concentric, external diameter 20mm

Coaxial nebulizer:Outer diameter 6mm

Double barrel atomizing chamber: Outer diameter 34mm

 

Gas Flow Controls

1. Plasma Argon Flowmeter:100-1000L/h (1.6-16L/min)

2. Auxiliary Argon Flowmeter:10-100L/h (0.16-1.66L/min)

3. Carrier Argon Flowmeter10-100L/h (0.16-1.66L/min)

4.Oxygen Flowmeter:0-100ml/min (30-50ml/min) 

5.Pressure Maintaining Valve0-0.4MPa

6.Cooling Water:Temperature: 20-25, Rate of Flow>5L/min, Hydraulic Pressure>0.1MPa

 

Spectrometer

Optics:Czerny-Turner type

Focal length: 1000 mm

Grating: Ion Beam Etching Holographic Grating, 4320L/mm

Reciprocal linear dispersion: 0.26nm/mm

Resolution: 0.005nm (4320 line grating)

Wavelength range: 4320 line grating:(180nm435) nm

Minimum pace of stepping motor: 0.0006 nm

Exit Slit:10μm;Entrance Slit:8μm

 

Photoelectric Converter Performance

Photomultiplier tube specification: R293

Negative HV on PMT: 0-1000V;Stability: 0.05%

 

Refrigeration System

Refrigerating Swirling Fog Chamber:The use of imported silica gel collection technology can make the temperature drop to 20 degrees below zero

 

Overall Performance

Wavelength range of scanning: 185nm435nm(4320L/mm line grating)

Repeatability: RSD(Relative Standard Deviation)1.5

Stability: RSD(Relative Standard Deviation) 2

Detection Limits (µg/L):

Direct injection sampling and measure iron(Fe), manganese(Mn), lead(Pb) and silicon(Si) in gasoline.Analysis results:

Element

Fe

Mn

Pb

Si

Determination value/(mg/L)

3.6

17.5

1.8

2.4

RSD/%

0.56

0.23

1.38

0.92

 

Standard Additionand Recovery Rate:

Number

Standard Addition

mg/L

Fe

Mn

Pb

Si

 

 

Determination valuemg/L

Recovery

/%

Determination valuemg/L

Recovery

/%

Determination valuemg/L

Recovery

/%

Determination valuemg/L

Recovery

/%

1

0.45

0.436

96.9

0.468

104.0

0.432

96.0

0.465

103.3

  2

0.9

0.887

98.6

0.913

101.4

0.868

96.4

0.919

102.1

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